This paper describes a modified synthesis of NaB3H8 by the reduction of BH3THF with sodium dispersed on silica gel. Single crystals obtained from CH2Cl2 show conclusively that the space group is Pmn21, in contrast to the Pmmn space group previously deduced from powder diffraction data.
ASJC Scopus subject areas
- Physical and Theoretical Chemistry
- Inorganic Chemistry