TY - JOUR
T1 - Synthesis and crystal structure of 5,10,15,20-tetrakis(3,5-dinitrophenyl)porphyrin
AU - Bhyrappa, P.
AU - Suslick, K. S.
PY - 1998
Y1 - 1998
N2 - The synthesis, characterization and crystal structure of the octanitro-substituted porphyrin 5,10,15,20-tetrakis(3,5-dinitrophenyl)porphyrin, H2T(3,5-DNP)P, are described. The solid state structure has two porphyrins in the unit cell with eight pyridine solvates and is made up from columnar arrays of the porphyrins. X-ray crystal structure data: monoclinic, space group P1 21/n1, a = 14.9996(9) Å, b = 8.2489(5) Å, c = 24.818(2) Å, α = 90°, β = 104.172(1)°, γ = 90°, V = 2977.3(3) Å3, dcalc = 1.440 g m-3, Z = 2.
AB - The synthesis, characterization and crystal structure of the octanitro-substituted porphyrin 5,10,15,20-tetrakis(3,5-dinitrophenyl)porphyrin, H2T(3,5-DNP)P, are described. The solid state structure has two porphyrins in the unit cell with eight pyridine solvates and is made up from columnar arrays of the porphyrins. X-ray crystal structure data: monoclinic, space group P1 21/n1, a = 14.9996(9) Å, b = 8.2489(5) Å, c = 24.818(2) Å, α = 90°, β = 104.172(1)°, γ = 90°, V = 2977.3(3) Å3, dcalc = 1.440 g m-3, Z = 2.
KW - Nitroporphyrin
KW - Structure determination
KW - Synthesis
KW - Tetraarylporphyrin
KW - Tetraphenylporphyrin
KW - X-ray crystallography
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U2 - 10.1002/(sici)1099-1409(199807/10)2:4/5<391::aid-jpp95>3.0.co;2-u
DO - 10.1002/(sici)1099-1409(199807/10)2:4/5<391::aid-jpp95>3.0.co;2-u
M3 - Article
AN - SCOPUS:3042983044
SN - 1088-4246
VL - 2
SP - 391
EP - 396
JO - Journal of Porphyrins and Phthalocyanines
JF - Journal of Porphyrins and Phthalocyanines
IS - 4-5
ER -