New one-pot method for the synthesis of alkynyl sulfonate esters using ultrasound

Atilla Tuncay; Beth M. Anaclerio; Melissa Zolodz; Kenneth S. Suslick

doi:10.1016/S0040-4039(98)02503-9

New one-pot method for the synthesis of alkynyl sulfonate esters using ultrasound

Atilla Tuncay, Beth M. Anaclerio, Melissa Zolodz, Kenneth S. Suslick

Research output: Contribution to journal › Article › peer-review

Abstract

A new one-pot method for the preparation of alkynyl sulfonate esters from terminal alkynes is reported. A metal-assisted, ultrasound-enhanced nucleophilic acetylenic displacement through the alkynyl(phenyl)iodonium salts provides a direct and rapid access to novel alkynyl sulfonates in good yields in a simple one-step procedure.

Original language	English (US)
Pages (from-to)	599-602
Number of pages	4
Journal	Tetrahedron Letters
Volume	40
Issue number	4
DOIs	https://doi.org/10.1016/S0040-4039(98)02503-9
State	Published - Jan 22 1999

Keywords

Alkynyl sulfonate esters
Hypervalent iodine
Sonochemistry
Ultrasound

ASJC Scopus subject areas

Biochemistry
Drug Discovery
Organic Chemistry

Online availability

10.1016/S0040-4039(98)02503-9

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title = "New one-pot method for the synthesis of alkynyl sulfonate esters using ultrasound",

abstract = "A new one-pot method for the preparation of alkynyl sulfonate esters from terminal alkynes is reported. A metal-assisted, ultrasound-enhanced nucleophilic acetylenic displacement through the alkynyl(phenyl)iodonium salts provides a direct and rapid access to novel alkynyl sulfonates in good yields in a simple one-step procedure.",

keywords = "Alkynyl sulfonate esters, Hypervalent iodine, Sonochemistry, Ultrasound",

author = "Atilla Tuncay and Anaclerio, {Beth M.} and Melissa Zolodz and Suslick, {Kenneth S.}",

note = "Funding Information: Acknowledgements: We thank the National Science Foundation (CHE-9420758) and Indiana University Northwest (Faculty Research Grant-in-Aid, Fellowships, and Undergraduate Research Fund) for financial support.",

year = "1999",

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doi = "10.1016/S0040-4039(98)02503-9",

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AU - Tuncay, Atilla

AU - Anaclerio, Beth M.

AU - Zolodz, Melissa

AU - Suslick, Kenneth S.

N1 - Funding Information: Acknowledgements: We thank the National Science Foundation (CHE-9420758) and Indiana University Northwest (Faculty Research Grant-in-Aid, Fellowships, and Undergraduate Research Fund) for financial support.

PY - 1999/1/22

Y1 - 1999/1/22

N2 - A new one-pot method for the preparation of alkynyl sulfonate esters from terminal alkynes is reported. A metal-assisted, ultrasound-enhanced nucleophilic acetylenic displacement through the alkynyl(phenyl)iodonium salts provides a direct and rapid access to novel alkynyl sulfonates in good yields in a simple one-step procedure.

AB - A new one-pot method for the preparation of alkynyl sulfonate esters from terminal alkynes is reported. A metal-assisted, ultrasound-enhanced nucleophilic acetylenic displacement through the alkynyl(phenyl)iodonium salts provides a direct and rapid access to novel alkynyl sulfonates in good yields in a simple one-step procedure.

KW - Alkynyl sulfonate esters

KW - Hypervalent iodine

KW - Sonochemistry

KW - Ultrasound

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U2 - 10.1016/S0040-4039(98)02503-9

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VL - 40

SP - 599

EP - 602

JO - Tetrahedron Letters

JF - Tetrahedron Letters

IS - 4

ER -

New one-pot method for the synthesis of alkynyl sulfonate esters using ultrasound

Abstract

Keywords

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