Microscale vacuum distillation apparatus for high-boiling, air- and heat-sensitive liquids

Sumeng Liu; Gregory S. Girolami

doi:10.1016/j.talanta.2020.121747

Microscale vacuum distillation apparatus for high-boiling, air- and heat-sensitive liquids

Research output: Contribution to journal › Article › peer-review

Abstract

We describe a simple apparatus that enables the vacuum distillation of ~0.2 mL of air- and water-sensitive, high-boiling liquids. The apparatus should be useful in teaching laboratories, and also to practicing chemists.

Original language	English (US)
Article number	121747
Journal	Talanta
Volume	223
DOIs	https://doi.org/10.1016/j.talanta.2020.121747
State	Published - Feb 1 2021
Externally published	Yes

Keywords

Air sensitive liquid
Microscale purification
Vacuum distillation

ASJC Scopus subject areas

Analytical Chemistry

Online availability

10.1016/j.talanta.2020.121747

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abstract = "We describe a simple apparatus that enables the vacuum distillation of ~0.2 mL of air- and water-sensitive, high-boiling liquids. The apparatus should be useful in teaching laboratories, and also to practicing chemists.",

keywords = "Air sensitive liquid, Microscale purification, Vacuum distillation",

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KW - Microscale purification

KW - Vacuum distillation

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Microscale vacuum distillation apparatus for high-boiling, air- and heat-sensitive liquids

Abstract

Keywords

ASJC Scopus subject areas

Online availability

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