In situ, high-temperature, synchrotron, powder diffraction studies of oxide systems in air, using a thermal-image furnace

L. F. Siah; W. M. Kriven; J. Schneider

doi:10.1088/0957-0233/16/6/008

In situ, high-temperature, synchrotron, powder diffraction studies of oxide systems in air, using a thermal-image furnace

L. F. Siah, W. M. Kriven, J. Schneider

Research output: Contribution to journal › Article › peer-review

Abstract

We have demonstrated the usefulness of employing a thermal-image furnace for in situ, high-temperature studies of oxide ceramics in air. Using Rietveld refinements lattice parameters and expansion coefficients can be measured up to 2000 °C in air. The use of an in situ temperature reference material is essential to monitor the sample temperature. Pt is effectively non-reactive with most oxide ceramics, which makes it an attractive in situ crystallographic 'thermometer' for studies at least up to 1550 °C; MgO and CeO₂ have been tested as internal thermometer materials for temperatures above 1550 °C.

Original language	English (US)
Pages (from-to)	1291-1298
Number of pages	8
Journal	Measurement Science and Technology
Volume	16
Issue number	6
DOIs	https://doi.org/10.1088/0957-0233/16/6/008
State	Published - Jun 1 2005

Keywords

High-temperature powder diffraction
Oxide ceramics
Thermal-image furnace

ASJC Scopus subject areas

Instrumentation
Engineering (miscellaneous)
Applied Mathematics

Online availability

10.1088/0957-0233/16/6/008

Library availability

Discover UIUC Full Text

Cite this

@article{61919b9fa7d34fb5affafb0aa29385e2,

title = "In situ, high-temperature, synchrotron, powder diffraction studies of oxide systems in air, using a thermal-image furnace",

abstract = "We have demonstrated the usefulness of employing a thermal-image furnace for in situ, high-temperature studies of oxide ceramics in air. Using Rietveld refinements lattice parameters and expansion coefficients can be measured up to 2000 °C in air. The use of an in situ temperature reference material is essential to monitor the sample temperature. Pt is effectively non-reactive with most oxide ceramics, which makes it an attractive in situ crystallographic 'thermometer' for studies at least up to 1550 °C; MgO and CeO2 have been tested as internal thermometer materials for temperatures above 1550 °C.",

keywords = "High-temperature powder diffraction, Oxide ceramics, Thermal-image furnace",

author = "Siah, {L. F.} and Kriven, {W. M.} and J. Schneider",

year = "2005",

month = jun,

day = "1",

doi = "10.1088/0957-0233/16/6/008",

language = "English (US)",

volume = "16",

pages = "1291--1298",

journal = "Measurement Science and Technology",

issn = "0957-0233",

publisher = "IOP Publishing Ltd.",

number = "6",

}

TY - JOUR

T1 - In situ, high-temperature, synchrotron, powder diffraction studies of oxide systems in air, using a thermal-image furnace

AU - Siah, L. F.

AU - Kriven, W. M.

AU - Schneider, J.

PY - 2005/6/1

Y1 - 2005/6/1

N2 - We have demonstrated the usefulness of employing a thermal-image furnace for in situ, high-temperature studies of oxide ceramics in air. Using Rietveld refinements lattice parameters and expansion coefficients can be measured up to 2000 °C in air. The use of an in situ temperature reference material is essential to monitor the sample temperature. Pt is effectively non-reactive with most oxide ceramics, which makes it an attractive in situ crystallographic 'thermometer' for studies at least up to 1550 °C; MgO and CeO2 have been tested as internal thermometer materials for temperatures above 1550 °C.

AB - We have demonstrated the usefulness of employing a thermal-image furnace for in situ, high-temperature studies of oxide ceramics in air. Using Rietveld refinements lattice parameters and expansion coefficients can be measured up to 2000 °C in air. The use of an in situ temperature reference material is essential to monitor the sample temperature. Pt is effectively non-reactive with most oxide ceramics, which makes it an attractive in situ crystallographic 'thermometer' for studies at least up to 1550 °C; MgO and CeO2 have been tested as internal thermometer materials for temperatures above 1550 °C.

KW - High-temperature powder diffraction

KW - Oxide ceramics

KW - Thermal-image furnace

UR - http://www.scopus.com/inward/record.url?scp=19944376499&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=19944376499&partnerID=8YFLogxK

U2 - 10.1088/0957-0233/16/6/008

DO - 10.1088/0957-0233/16/6/008

M3 - Article

AN - SCOPUS:19944376499

SN - 0957-0233

VL - 16

SP - 1291

EP - 1298

JO - Measurement Science and Technology

JF - Measurement Science and Technology

IS - 6

ER -

In situ, high-temperature, synchrotron, powder diffraction studies of oxide systems in air, using a thermal-image furnace

Abstract

Keywords

ASJC Scopus subject areas

Online availability

Library availability

Related links

Fingerprint

Cite this