Hydroxylammonium nitrate species in a monopropellant electrospray plume

Mitchell J. Wainwright, Joshua L. Rovey, Shawn W. Miller, Benjamin D. Prince, Steven P. Berg

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Abstract

A mixture of 1-ethyl-3-methylimidazolium ethyl sulfate ([Emim][EtSO4]) and hydroxylammonium nitrate (HAN) is an energetic monopropellant potentially suitable in a multi-mode chemical-electric microtube-electrospray micropropulsion system. In this work, electrospray plume mass spectra are compared between the monopropellant mixture and neat [Emim][EtSO4]. This comparison clearly indicates new and additional species present in the plume due to the addition of HAN. Mass spectra from 20-600 amu/q were obtained over a variety of angles and flow rates from 2 pL/sec to 3 nL/sec in both cation and anion extraction modes. Mass spectrum dependence on flow rate and angular orientation agree qualitatively well with literature. Results indicate the presence of HAN-based species in anion mode, but no HAN-based species in cation mode. Three of the four monomer species from the monopropellant are apparent in the plume; [Emim]+, [EtSO4]-, and [NO3]- are observed, while [HA]+ is noticeably absent. Results also show emission of both protontransferred covalent forms of HAN: [HA-H] and [HNO3]. Swapping of anion and cation species between the constituents of the monopropellant mixture is also observed.

Original languageEnglish (US)
Title of host publicationAIAA Propulsion and Energy Forum and Exposition, 2019
PublisherAmerican Institute of Aeronautics and Astronautics Inc, AIAA
ISBN (Print)9781624105906
DOIs
StatePublished - 2019
Externally publishedYes
EventAIAA Propulsion and Energy Forum and Exposition, 2019 - Indianapolis, United States
Duration: Aug 19 2019Aug 22 2019

Publication series

NameAIAA Propulsion and Energy Forum and Exposition, 2019

Conference

ConferenceAIAA Propulsion and Energy Forum and Exposition, 2019
Country/TerritoryUnited States
CityIndianapolis
Period8/19/198/22/19

ASJC Scopus subject areas

  • General Energy
  • Aerospace Engineering
  • Electrical and Electronic Engineering
  • Control and Systems Engineering
  • Mechanical Engineering

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