High resolution solid-state n.m.r. studies of quadrupolar nuclei: Quadrupole-induced shifts in variable-angle sample-spinning of a borosilicate glass

Suzanne Schramm; Eric Oldfield

doi:10.1039/c39820000980

High resolution solid-state n.m.r. studies of quadrupolar nuclei: Quadrupole-induced shifts in variable-angle sample-spinning of a borosilicate glass

Suzanne Schramm, Eric Oldfield

Chemistry

Research output: Contribution to journal › Article › peer-review

Abstract

We report the first observation of field-dependent quadrupole-induced shifts in variable-angle sample-spinning n.m.r. spectra of the ¹¹B nucleus (l = 3/2) in a borosilicate glass: the results indicate that differences in electric quadrupole coupling constant may be used in variable-angle sample-spinning n.m.r. studies at low magnetic field strengths to provide highly resolved spectra of some non-integral spin quadrupolar nuclei.

Original language	English (US)
Pages (from-to)	980-981
Number of pages	2
Journal	Journal of the Chemical Society, Chemical Communications
Issue number	17
DOIs	https://doi.org/10.1039/c39820000980
State	Published - 1982

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Molecular Medicine

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10.1039/c39820000980

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abstract = "We report the first observation of field-dependent quadrupole-induced shifts in variable-angle sample-spinning n.m.r. spectra of the 11B nucleus (l = 3/2) in a borosilicate glass: the results indicate that differences in electric quadrupole coupling constant may be used in variable-angle sample-spinning n.m.r. studies at low magnetic field strengths to provide highly resolved spectra of some non-integral spin quadrupolar nuclei.",

author = "Suzanne Schramm and Eric Oldfield",

year = "1982",

doi = "10.1039/c39820000980",

language = "English (US)",

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journal = "Chemical Communications",

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publisher = "Royal Society of Chemistry",

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AU - Oldfield, Eric

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N2 - We report the first observation of field-dependent quadrupole-induced shifts in variable-angle sample-spinning n.m.r. spectra of the 11B nucleus (l = 3/2) in a borosilicate glass: the results indicate that differences in electric quadrupole coupling constant may be used in variable-angle sample-spinning n.m.r. studies at low magnetic field strengths to provide highly resolved spectra of some non-integral spin quadrupolar nuclei.

AB - We report the first observation of field-dependent quadrupole-induced shifts in variable-angle sample-spinning n.m.r. spectra of the 11B nucleus (l = 3/2) in a borosilicate glass: the results indicate that differences in electric quadrupole coupling constant may be used in variable-angle sample-spinning n.m.r. studies at low magnetic field strengths to provide highly resolved spectra of some non-integral spin quadrupolar nuclei.

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High resolution solid-state n.m.r. studies of quadrupolar nuclei: Quadrupole-induced shifts in variable-angle sample-spinning of a borosilicate glass

Abstract

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