High resolution solid-state n.m.r. studies of quadrupolar nuclei: Quadrupole-induced shifts in variable-angle sample-spinning of a borosilicate glass

Suzanne Schramm, Eric Oldfield

Research output: Contribution to journalArticlepeer-review

Abstract

We report the first observation of field-dependent quadrupole-induced shifts in variable-angle sample-spinning n.m.r. spectra of the 11B nucleus (l = 3/2) in a borosilicate glass: the results indicate that differences in electric quadrupole coupling constant may be used in variable-angle sample-spinning n.m.r. studies at low magnetic field strengths to provide highly resolved spectra of some non-integral spin quadrupolar nuclei.

Original languageEnglish (US)
Pages (from-to)980-981
Number of pages2
JournalJournal of the Chemical Society, Chemical Communications
Issue number17
DOIs
StatePublished - Jan 1 1982

ASJC Scopus subject areas

  • Molecular Medicine

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