@article{54686de777aa4d2c9ad00eb76e5a9949,
title = "Dislocation cells in additively manufactured metallic alloys characterized by electron backscatter diffraction pattern sharpness",
abstract = "Metallic alloys produced by additive manufacturing often host complex and hierarchical microstructures with grains exhibiting large orientation gradients, along with sub-grain dislocation cells. These multiscale features act in concert to control mechanical behavior, yet are challenging to characterize at high fidelity over large areas. Here, we quantify the sharpness of electron backscatter diffraction patterns obtained from several additively manufactured metallic alloys to directly image the dislocation cells at the mesoscale in bulk materials. The sharpness metric employed herein reflects the elastic strain field from dislocations, and exhibits unique advantages, including being proportional to local dislocation density, insensitive to grain orientation, and inherently correlated with orientation mapping and its related modalities. Our results demonstrate that the cell walls do not always possess appreciable misorientations, and thus do not always contain large fractions of geometrically necessary dislocations, thereby furthering our understanding of the origin and implications of the profuse dislocation cells produced during additive manufacturing.",
keywords = "Additive manufacturing, Dislocation cell, Electron backscattering diffraction (EBSD), Metal and alloys, Microstructure",
author = "Fulin Wang and Stinville, {Jean Charles} and Marie Charpagne and Echlin, {McLean P.} and Agnew, {Sean R.} and Pollock, {Tresa M.} and Graef, {Marc De} and Gianola, {Daniel S.}",
note = "Funding Information: F. Wang gratefully acknowledges the support of Shanghai Pujiang Program (No. 21PJ1406700). This work was supported by the Materials Research Science and Engineering Center (MRSEC) program of the National Science Foundation (NSF) through DMR-1720256 (IRG-1), and employed the shared facilities of the MRSEC at UC Santa Barbara, a member of the Materials Research Facilities Network. We also acknowledge support from the Major Research Instrumentation Awards NSFDMR-1828628 and DMR-2117843. Use was made of the computational facilities administered by the Center for Scientific Computing at the CNSI and MRL (an NSF MRSEC; DMR-1720256) and purchased through NSF CNS-1725797. Furthermore, GPU resources through NSF CC* Compute 1925717 were also leveraged. MDG acknowledges funding from a DoD Vannevar-Bush Faculty Fellowship (N00014-16–1-2821). We thank Benjamin Bammes and Barnaby Levin (Direct Electron) for instrument support and fruitful discussions. Funding Information: F. Wang gratefully acknowledges the support of Shanghai Pujiang Program (No. 21PJ1406700 ). This work was supported by the Materials Research Science and Engineering Center (MRSEC) program of the National Science Foundation (NSF) through DMR-1720256 (IRG-1), and employed the shared facilities of the MRSEC at UC Santa Barbara, a member of the Materials Research Facilities Network. We also acknowledge support from the Major Research Instrumentation Awards NSF DMR-1828628 and DMR-2117843 . Use was made of the computational facilities administered by the Center for Scientific Computing at the CNSI and MRL (an NSF MRSEC; DMR-1720256) and purchased through NSF CNS-1725797. Furthermore, GPU resources through NSF CC* Compute 1925717 were also leveraged. MDG acknowledges funding from a DoD Vannevar-Bush Faculty Fellowship (N00014-16–1-2821). We thank Benjamin Bammes and Barnaby Levin (Direct Electron) for instrument support and fruitful discussions. Publisher Copyright: {\textcopyright} 2023 Elsevier Inc.",
year = "2023",
month = mar,
doi = "10.1016/j.matchar.2023.112673",
language = "English (US)",
volume = "197",
journal = "Materials Characterization",
issn = "1044-5803",
publisher = "Elsevier Inc.",
}