A high-yield route to 1,2-dihydrocyclobutazene-3,6-dicarboxylic acid

K. A. Walker, L. J. Markoski, J. S. Moore

Research output: Contribution to journalArticle

Abstract

A simple five-step method for preparing the previously unknown 1.2-dihydrocyclobutabenzene-3,6-dicarboxylic acid (XTA) in high yield is presented. All intermediates were crystalline compounds which allowed the preparation to be scaled up without complication. The title compound is of interest as a crosslinkable derivative of the widely used monomer, terephthalic acid (TA).

Original languageEnglish (US)
Pages (from-to)1265-1268
Number of pages4
JournalSynthesis
Issue number12
DOIs
StatePublished - Jan 1 1992
Externally publishedYes

ASJC Scopus subject areas

  • Catalysis
  • Organic Chemistry

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