A general protocol for temperature calibration of MAS NMR probes at arbitrary spinning speeds

Keyphrases

• MAS NMR 100%
• NMR Probe 100%
• Spinning Speed 100%
• Temperature Calibration 100%
• Magic Angle Spinning 50%
• Empirical Formula 50%
• Sample Temperature 50%
• Temperature Setpoint 50%
• Nominal Sets 50%
• Typical Sample 50%
• Spinning Rate 50%
• 207Pb 50%
• Lead Nitrate 50%

Engineering

• Temperature Calibration 100%
• Sample Temperature 50%
• Set Temperature 50%