A general protocol for temperature calibration of MAS NMR probes at arbitrary spinning speeds

Xudong Guan, Ruth E. Stark

Research output: Contribution to journalArticle

Abstract

A protocol using 207Pb NMR of solid lead nitrate was developed to determine the temperature of magic-angle spinning (MAS) NMR probes over a range of nominal set temperatures and spinning speeds. Using BioMAS and FastMAS probes with typical sample spinning rates of 8 and 35 kHz, respectively, empirical equations were devised to predict the respective sample temperatures. These procedures provide a straightforward recipe for temperature calibration of any MAS probe.

Original languageEnglish (US)
Pages (from-to)74-76
Number of pages3
JournalSolid State Nuclear Magnetic Resonance
Volume38
Issue number2-3
DOIs
StatePublished - Sep 1 2010
Externally publishedYes

Fingerprint

Magic angle spinning
metal spinning
Nuclear magnetic resonance
Calibration
nuclear magnetic resonance
probes
Temperature
temperature
nitrates
Nitrates
Lead

Keywords

  • Magic-angle spinning
  • Pb NMR
  • Temperature calibration

ASJC Scopus subject areas

  • Radiation
  • Chemistry(all)
  • Nuclear and High Energy Physics
  • Instrumentation

Cite this

A general protocol for temperature calibration of MAS NMR probes at arbitrary spinning speeds. / Guan, Xudong; Stark, Ruth E.

In: Solid State Nuclear Magnetic Resonance, Vol. 38, No. 2-3, 01.09.2010, p. 74-76.

Research output: Contribution to journalArticle

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