A general protocol for temperature calibration of MAS NMR probes at arbitrary spinning speeds

Xudong Guan; Ruth E. Stark

doi:10.1016/j.ssnmr.2010.10.001

A general protocol for temperature calibration of MAS NMR probes at arbitrary spinning speeds

Xudong Guan, Ruth E. Stark

Carl R. Woese Institute for Genomic Biology

Research output: Contribution to journal › Article

Abstract

A protocol using ²⁰⁷Pb NMR of solid lead nitrate was developed to determine the temperature of magic-angle spinning (MAS) NMR probes over a range of nominal set temperatures and spinning speeds. Using BioMAS and FastMAS probes with typical sample spinning rates of 8 and 35 kHz, respectively, empirical equations were devised to predict the respective sample temperatures. These procedures provide a straightforward recipe for temperature calibration of any MAS probe.

Original language	English (US)
Pages (from-to)	74-76
Number of pages	3
Journal	Solid State Nuclear Magnetic Resonance
Volume	38
Issue number	2-3
DOIs	https://doi.org/10.1016/j.ssnmr.2010.10.001
State	Published - Sep 1 2010

Keywords

Magic-angle spinning
Pb NMR
Temperature calibration

ASJC Scopus subject areas

Radiation
Chemistry(all)
Nuclear and High Energy Physics
Instrumentation

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10.1016/j.ssnmr.2010.10.001

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Guan, X., & Stark, R. E. (2010). A general protocol for temperature calibration of MAS NMR probes at arbitrary spinning speeds. Solid State Nuclear Magnetic Resonance, 38(2-3), 74-76. https://doi.org/10.1016/j.ssnmr.2010.10.001

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