Abstract
A protocol using 207Pb NMR of solid lead nitrate was developed to determine the temperature of magic-angle spinning (MAS) NMR probes over a range of nominal set temperatures and spinning speeds. Using BioMAS and FastMAS probes with typical sample spinning rates of 8 and 35 kHz, respectively, empirical equations were devised to predict the respective sample temperatures. These procedures provide a straightforward recipe for temperature calibration of any MAS probe.
| Original language | English (US) |
|---|---|
| Pages (from-to) | 74-76 |
| Number of pages | 3 |
| Journal | Solid State Nuclear Magnetic Resonance |
| Volume | 38 |
| Issue number | 2-3 |
| DOIs | |
| State | Published - Sep 1 2010 |
| Externally published | Yes |
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Keywords
- Magic-angle spinning
- Pb NMR
- Temperature calibration
ASJC Scopus subject areas
- Radiation
- Chemistry(all)
- Nuclear and High Energy Physics
- Instrumentation
Cite this
A general protocol for temperature calibration of MAS NMR probes at arbitrary spinning speeds. / Guan, Xudong; Stark, Ruth E.
In: Solid State Nuclear Magnetic Resonance, Vol. 38, No. 2-3, 01.09.2010, p. 74-76.Research output: Contribution to journal › Article
}
TY - JOUR
T1 - A general protocol for temperature calibration of MAS NMR probes at arbitrary spinning speeds
AU - Guan, Xudong
AU - Stark, Ruth E.
PY - 2010/9/1
Y1 - 2010/9/1
N2 - A protocol using 207Pb NMR of solid lead nitrate was developed to determine the temperature of magic-angle spinning (MAS) NMR probes over a range of nominal set temperatures and spinning speeds. Using BioMAS and FastMAS probes with typical sample spinning rates of 8 and 35 kHz, respectively, empirical equations were devised to predict the respective sample temperatures. These procedures provide a straightforward recipe for temperature calibration of any MAS probe.
AB - A protocol using 207Pb NMR of solid lead nitrate was developed to determine the temperature of magic-angle spinning (MAS) NMR probes over a range of nominal set temperatures and spinning speeds. Using BioMAS and FastMAS probes with typical sample spinning rates of 8 and 35 kHz, respectively, empirical equations were devised to predict the respective sample temperatures. These procedures provide a straightforward recipe for temperature calibration of any MAS probe.
KW - Magic-angle spinning
KW - Pb NMR
KW - Temperature calibration
UR - http://www.scopus.com/inward/record.url?scp=78649475837&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=78649475837&partnerID=8YFLogxK
U2 - 10.1016/j.ssnmr.2010.10.001
DO - 10.1016/j.ssnmr.2010.10.001
M3 - Article
C2 - 21036557
AN - SCOPUS:78649475837
VL - 38
SP - 74
EP - 76
JO - Solid State Nuclear Magnetic Resonance
JF - Solid State Nuclear Magnetic Resonance
SN - 0926-2040
IS - 2-3
ER -